By Gehman H. M.
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However, decreasing the hydrogen fluoride from 50 to 14 equivalents not only reduces the yield and selectivity towards the p-aldehyde, but a substantial increase in secondary product formation was observed. 14 eq) is evident from the drop in the p-aldehyde yield to 3%. This result confirmed the important facilitating role of the Lewis acid. 2 Run 4) Since near-supercritical water may act as an acid205, it offers an environmentally benevolent alternative for the replacement of undesirable solvents and catalysts and may potentially assist in the formylation of aromatic aldehydes using carbon monoxide.
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A Special Type of Upper Semi-Continuous Collection by Gehman H. M.